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On August 4, 2023 at 9:04:09 AM UTC,
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f | 1 | { | f | 1 | { |
2 | "author": "Melinte, Georgian", | 2 | "author": "Melinte, Georgian", | ||
3 | "author_email": "", | 3 | "author_email": "", | ||
4 | "creator_user_id": "17755db4-395a-4b3b-ac09-e8e3484ca700", | 4 | "creator_user_id": "17755db4-395a-4b3b-ac09-e8e3484ca700", | ||
5 | "doi": "10.35097/1310", | 5 | "doi": "10.35097/1310", | ||
6 | "doi_date_published": "2023", | 6 | "doi_date_published": "2023", | ||
7 | "doi_publisher": "", | 7 | "doi_publisher": "", | ||
8 | "doi_status": "True", | 8 | "doi_status": "True", | ||
9 | "groups": [], | 9 | "groups": [], | ||
10 | "id": "dfead70f-88af-4b91-af73-5148e1333015", | 10 | "id": "dfead70f-88af-4b91-af73-5148e1333015", | ||
11 | "isopen": false, | 11 | "isopen": false, | ||
12 | "license_id": "CC BY-NC 4.0 Attribution-NonCommercial", | 12 | "license_id": "CC BY-NC 4.0 Attribution-NonCommercial", | ||
13 | "license_title": "CC BY-NC 4.0 Attribution-NonCommercial", | 13 | "license_title": "CC BY-NC 4.0 Attribution-NonCommercial", | ||
14 | "metadata_created": "2023-08-04T08:50:30.091787", | 14 | "metadata_created": "2023-08-04T08:50:30.091787", | ||
t | 15 | "metadata_modified": "2023-08-04T08:53:28.216987", | t | 15 | "metadata_modified": "2023-08-04T09:04:09.861736", |
16 | "name": "rdr-doi-10-35097-1310", | 16 | "name": "rdr-doi-10-35097-1310", | ||
17 | "notes": "TechnicalRemarks: The data contains Digital Micrograph | 17 | "notes": "TechnicalRemarks: The data contains Digital Micrograph | ||
18 | files in the .dm3 and .dm4 formats and Velox files in the .vmd format. | 18 | files in the .dm3 and .dm4 formats and Velox files in the .vmd format. | ||
19 | Digital Micrograph (DM) data can be open either by installing the | 19 | Digital Micrograph (DM) data can be open either by installing the | ||
20 | offline and free version of the DM software from the Gatan website or | 20 | offline and free version of the DM software from the Gatan website or | ||
21 | by using the open access Fiji software. Velox data can be open with a | 21 | by using the open access Fiji software. Velox data can be open with a | ||
22 | special script available for DM.\r\nExperimental details: \r\nIn order | 22 | special script available for DM.\r\nExperimental details: \r\nIn order | ||
23 | to perform TEM measurements the sample was prepared inside an argon | 23 | to perform TEM measurements the sample was prepared inside an argon | ||
24 | field glovebox and then transferred to the microscope using a vacuum | 24 | field glovebox and then transferred to the microscope using a vacuum | ||
25 | transfer holder in order to prevent samples from extensive air | 25 | transfer holder in order to prevent samples from extensive air | ||
26 | exposure. The dry powder of the samples was directly dispersed on the | 26 | exposure. The dry powder of the samples was directly dispersed on the | ||
27 | TEM holey carbon membrane without the use of solvents. The | 27 | TEM holey carbon membrane without the use of solvents. The | ||
28 | measurements were performed using a double aberration corrected and | 28 | measurements were performed using a double aberration corrected and | ||
29 | monochromated Themis Z microscope equipped with a Gatan GIF Continuum | 29 | monochromated Themis Z microscope equipped with a Gatan GIF Continuum | ||
30 | 970 spectrometer and a K3 IS camera. High-resolution STEM-HAADF | 30 | 970 spectrometer and a K3 IS camera. High-resolution STEM-HAADF | ||
31 | images were recorded using a collection angle range of 63-200mrad. | 31 | images were recorded using a collection angle range of 63-200mrad. | ||
32 | EELS spectrum imaging data cubes were acquired with a probe | 32 | EELS spectrum imaging data cubes were acquired with a probe | ||
33 | convergence angle of 30 mrad and a probe current of 0.5nA. The pixel | 33 | convergence angle of 30 mrad and a probe current of 0.5nA. The pixel | ||
34 | size was around 1 nm and a dwell time of 0.1s per pixel for all the | 34 | size was around 1 nm and a dwell time of 0.1s per pixel for all the | ||
35 | data series. The camera length was 30 mm and the spectrometer aperture | 35 | data series. The camera length was 30 mm and the spectrometer aperture | ||
36 | was set to 5 mm resulting in a collection angle of about 40 mrad. All | 36 | was set to 5 mm resulting in a collection angle of about 40 mrad. All | ||
37 | EELS data was acquired in dual-EELS mode containing both the core loss | 37 | EELS data was acquired in dual-EELS mode containing both the core loss | ||
38 | and the low loss spectra. All core loss spectra were realigned and | 38 | and the low loss spectra. All core loss spectra were realigned and | ||
39 | deconvoluted based on the low loss spectra pairs prior to any data | 39 | deconvoluted based on the low loss spectra pairs prior to any data | ||
40 | analysis.", | 40 | analysis.", | ||
41 | "num_resources": 0, | 41 | "num_resources": 0, | ||
42 | "num_tags": 0, | 42 | "num_tags": 0, | ||
43 | "orcid": "", | 43 | "orcid": "", | ||
44 | "organization": { | 44 | "organization": { | ||
45 | "approval_status": "approved", | 45 | "approval_status": "approved", | ||
46 | "created": "2023-01-12T13:30:23.238233", | 46 | "created": "2023-01-12T13:30:23.238233", | ||
47 | "description": "RADAR (Research Data Repository) is a | 47 | "description": "RADAR (Research Data Repository) is a | ||
48 | cross-disciplinary repository for archiving and publishing research | 48 | cross-disciplinary repository for archiving and publishing research | ||
49 | data from completed scientific studies and projects. The focus is on | 49 | data from completed scientific studies and projects. The focus is on | ||
50 | research data from subjects that do not yet have their own | 50 | research data from subjects that do not yet have their own | ||
51 | discipline-specific infrastructures for research data management. ", | 51 | discipline-specific infrastructures for research data management. ", | ||
52 | "id": "013c89a9-383c-4200-8baa-0f78bf1d91f9", | 52 | "id": "013c89a9-383c-4200-8baa-0f78bf1d91f9", | ||
53 | "image_url": "radar-logo.svg", | 53 | "image_url": "radar-logo.svg", | ||
54 | "is_organization": true, | 54 | "is_organization": true, | ||
55 | "name": "radar", | 55 | "name": "radar", | ||
56 | "state": "active", | 56 | "state": "active", | ||
57 | "title": "RADAR", | 57 | "title": "RADAR", | ||
58 | "type": "organization" | 58 | "type": "organization" | ||
59 | }, | 59 | }, | ||
60 | "owner_org": "013c89a9-383c-4200-8baa-0f78bf1d91f9", | 60 | "owner_org": "013c89a9-383c-4200-8baa-0f78bf1d91f9", | ||
61 | "private": false, | 61 | "private": false, | ||
62 | "production_year": "2021", | 62 | "production_year": "2021", | ||
63 | "publication_year": "2023", | 63 | "publication_year": "2023", | ||
64 | "publishers": [ | 64 | "publishers": [ | ||
65 | { | 65 | { | ||
66 | "publisher": "Karlsruhe Institute of Technology" | 66 | "publisher": "Karlsruhe Institute of Technology" | ||
67 | } | 67 | } | ||
68 | ], | 68 | ], | ||
69 | "relationships_as_object": [], | 69 | "relationships_as_object": [], | ||
70 | "relationships_as_subject": [], | 70 | "relationships_as_subject": [], | ||
71 | "repository_name": "RADAR (Research Data Repository)", | 71 | "repository_name": "RADAR (Research Data Repository)", | ||
72 | "resources": [], | 72 | "resources": [], | ||
73 | "services_used_list": "", | 73 | "services_used_list": "", | ||
74 | "source_metadata_created": "2023", | 74 | "source_metadata_created": "2023", | ||
75 | "source_metadata_modified": "", | 75 | "source_metadata_modified": "", | ||
76 | "state": "active", | 76 | "state": "active", | ||
77 | "subject_areas": [ | 77 | "subject_areas": [ | ||
78 | { | 78 | { | ||
79 | "subject_area_additional": "", | 79 | "subject_area_additional": "", | ||
80 | "subject_area_name": "Engineering" | 80 | "subject_area_name": "Engineering" | ||
81 | } | 81 | } | ||
82 | ], | 82 | ], | ||
83 | "tags": [], | 83 | "tags": [], | ||
84 | "title": "Tem original data of the lno (pristine and heat treated) | 84 | "title": "Tem original data of the lno (pristine and heat treated) | ||
85 | samples", | 85 | samples", | ||
86 | "type": "vdataset", | 86 | "type": "vdataset", | ||
87 | "url": "https://doi.org/10.35097/1310" | 87 | "url": "https://doi.org/10.35097/1310" | ||
88 | } | 88 | } |